Determination of trilostane by hplc
WebTrilostane inhibits synthesis of cortisol in dogs. It is a competitive inhibitor of 3-beta-hydroxysteroid dehydrogenate, which will interfere with the steps that lead to cortisol … WebIn view of the problems described in the Reference Example in relation to the degradation of Trilostane on a silica-based stationary phase, an improved HPLC system, described …
Determination of trilostane by hplc
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WebMar 6, 2016 · The optimized HPLC method was validated, and based on the results obtained, it is found that the proposed method is linear, precise and accurate. Validation data also demonstrate that this method can be used in routine analysis of potassium sorbate, sodium benzoate, quinoline yellow and sunset yellow in lemonades and lemon … WebMay 7, 2012 · Figure 2 shows a typical chromatogram of a working sample solution obtained under the optimized HPLC conditions described in the preceding. The amino-bonded silica packing has been widely used for the separation of carbohydrates. When used in the current study, it provided the required separation of sorbitol and glycerol from each other and …
WebHigh pressure liquid chromatographic (HPLC) analysis of plasma taken over 8 h from ten normal male subjects medicated with 120 mg of trilostane revealed that the drug is rapidly metabolised into at least one metabolite, 17-keto trilostane. Both compounds were detected in the blood stream at concentr … WebA trilostane assay was developed using reagents and chemicals of high-performance liquid chromatography (HPLC) analytical grade. An Agilent 1260 Infinity HPLC system (Santa Clara, California) equipped with a pump (model G7111A), an auto sampler (model G7129A), Kinetex C18 (150 4.6 mm, 5 μm particle size) column (Torrance, Cali-
WebJun 1, 2002 · Abstract and Figures. An isocratic reversed-phase liquid chromatographic (HPLC) method is proposed for the practical and reliable determination of triclosan, an … http://jcore-reference.highwire.org/content/48/4/228
WebGas chromatography (GC) and high-performance liquid chromatography (HPLC) coupled to different detectors, and in combination with different sample extraction methods, are most widely used for analysis of triazine herbicides in different environmental samples. Nowadays, many variations and modificati …
WebJan 1, 2011 · A new method for analysis of benzene, toluene, and xylene (BTX) using High Performance Liquid Chromatography-UV detection (HPLC-UV) is described and compared to the gas chromatography (GC) method. highlight anchor links on scrollWebA trilostane assay was developed for analysis. Trilostane (Vetoryl) capsules were used as clinical controls. Forty-four medication packets containing trilostane (Vetoryl), prepared … small money safe boxWebThus, plasma analysis is required to support in vivo studies in rats designed to maximise absorption. Two high-performance liquid chromatographic (HPLC) assays for trilostane … small money safe fireproofWebJun 14, 1991 · A simple high-performance liquid chromatographic (HPLC) method for assaying trilostane, a synthetic steroid, and one of its metabolites, ketotrilostane, in small volumes of rat plasma has been developed. A single liquid-liquid extraction was used to … highlight alternate rows in excelWebThe Newcrom columns are a family of reverse phase-based columns. Newcrom A, AH, B, and BH are all mixed-mode columns with either positive or negative ion-pairing groups … small money safe with keyWebWater samples were collected from each tank every 2–3 days (9/21 days in total) and trilostane concentrations in the water were measured by high-performance liquid chromatography (HPLC) with diode array detection (254 nm; Model 1100; Agilent Techologies, Santa Clara, CA). The HPLC was equipped with a Zorbax SB-C18 column … highlight amsterdamWebJul 30, 2024 · Analytical method for the quantitative determination of EDTA in Cosmetics has been developed and validated by high-performance liquid chromatography (HPLC) with UV detection at wavelength 280 nm. small money tin